摘要:An efficient radioimmunoassay for determination of the physiological level of progesterone in human serum was developed, using 3H-labelled progesterone as radiologand and progesterone-11α-succinyl-BSA as immunogen. It was applied to determine the serum progesterone level of women in regular menstruation in second trimester of pregnancy and administration of the aborfifacient.
摘要:The absolute intensity of medical isotopes 131I and 198Au with a short half-life has been measured by the efficiency extrapolation method of 4πβ-γ coincidence absorption curve. The result of the measurement has been corrected for background, dead time, resolving time respectively. The correction for the short half-life has also been considered. The maximum error of the measurement are 0.57% and 1.7% for 131I and 198Au respectively. After a little change of the apparatus, we have measured the nuclide with electron capture decay.
摘要:This paper describes a method of measuring the depth and concentraction of impurity layer using nuclear reaction analysis. The phosphorus in silicon was bombarded by low energy proton beam. The depth and concentraction of phosphorus layer in monocrystalline silicon was measured by the yield curves of 31P (p, α)28Si resonance reaction, and the errors in experiment were discussed.
摘要:The graft copolymerization of Methacrylic acid-divinylbenzene mixed monomers from its aqueous solution onto pre-irradiated F46 film was studied in detail. The total dose of electron beam pre-irradiation laid between the range of (3~8) ×105rad and the reaction temperature was 80~95℃. The duration for graft copolymerization various with the total absorbed dose and reaction temperature.The optimum composition of aqueous solution of mixed monomers was obtained from the phase diagram of Methacrylic acid-divinylbenzene-H2O ternary system therefore constructed.The resulting grafts can give cation exchange membranes with excellent electrochemical properties and high mechanical strength.The membranes have following major characteristics:1. Ion exchange Capacity (IEC) 2~3 meq/g2.Specific resistance (ρ) 50~100 Ω-cm3.permselectivity 95~98%4. Tensile strength ≥160kg/cm2
Liu Shu-lin,Zhang Li-min,Wang Ling-zhen,Zhou Zhi-gen
1981, 04(1)
摘要:The X-ray exposures in unit of C.kg-1 or Röentgen were measured by a parallel—plate free air ionization chamber. The plate distance was 20.9cm. The length of collector was 10cm. The correction factors were determined. The uncertainty of measurement was about 1.8% for 60~250kV X-rays. The long-term standard deviation was ±0.1%.
摘要:It is sometimes necessary to monitor and control the thicknees of a film during the process of vacuum evaporation. This paper describes a quartz oscillator for this purpose. It is based on the frequency variation caused by the change in thickness of crystal surface. The calibrations for frequency variation per unit thicknees have been performed using six elements of Pb, Bi, Cu, Au, Al, and Ag.
摘要:Two resins with chelating group of made by Nankai university were used. Adsorptions of Rhodinium and Iridium on resins were measured unde static conditions at different concentration of HCl at room temperature and 100℃ using 101mRh and 192Ir as indicators. The adsorption reached >80% for RhIII and >90% for IrIV at optimal conditions. It was found that these chelating resins have higher selectivity for noble metals than most of other metal ions. (Al3+, Fe3+, Cu2+, Co2+, Ni2+ etc.)
摘要:The exposure in a radiation field with a large-scale extended radiation source and its theoretical estimation is shortly described in this paper. The theoretical values are in good agreement with the measurements. In case of a plate-type radiation source made up of putting numerous cobalt rods together, the distribution theory on field strength of extended radiation source may be used to evaluate the exposure distribution in the radiation field and, therefore, to obtain the places at which the dose in demanded. The relative error between the theorical and measured values is in general less than 9%.
摘要:Nitrogen was determined in Ta and Nb with charged particle Activation Analysis. The 14O activity from the reaction 14N (p, n)14O is produced by a beam of protons of 7.0 MeV. After chemical etching, the 14O activity (Eγ=2.313 MeV) of the sample was measured by means of a Ge(Li) or NaI(T1) detector. The half-life of 14O is 70.5sec. The analysis is nondestructive, and interferences do not arise. This method gives sensitivities of 0.5 and 6µg · g-1 for the analysis of Ta and Nb, respectively. Each analysis lasts about 5min. The method is applicable to determine trace nitrogen without chemical separation.