摘要:he hardness values of Cr12MoV steel before and after N+ and Mo-implantation were measured. AES was used to determine the chemical composition ofthe implanted layers and the metallographic analysis was conducted. The effect of N+and Mo+ implantation on hardness of Cr12MoV steel was discussed.
摘要:Two methods for preparing 15-(p-125I iodophenyl)-pentadecanoic acid werecompared. Within one hour IPPA can be easily labelled with 125I by theiodine-isotope exchange. In contrast to the direct labelling method of PPA, thismethod gives a 70% radio-chemical yield and the product with high purity.
摘要:This paper describes a new way, the Two-peak Method, in which both thelow-temperature peak and the high--temperature peak in a TL glow curve are usedfor age determination. This method is useful in overcoming the difficulties arisingfrom the fact that parallel samples may have different TL response at a singletemperature peak.
摘要:Post-treatment such as electron beam heating and thermal annealing, was usedfor the r.f. magnetron sputtering deposited ZrO2-12wt%Y2O3 films. Studies on phasecomposition, oxidized states of Zr, and characterized morphologies of the films beforeand after post-treatment were made with SEM, XRD and XPS, and the selection ofpost treatment to increase film’s durability was also discussed.
摘要:The self-burial process of a parabolic nuclear waste container, which releasesheat and melts its way through the surroundings in the direction of gravity, isstudied. The heat transfer and motion of the liquid melted in front of the containerare analysed by the film theory. The surface temperature and self-burial rate of thecontainer are derived, and some influential factors are discussed.
关键词:Phase change phenomena;Nuclear waste disposal;Heat transfer
摘要:The structure and measurement principle of a heat-loss-compensated aluminiumabsorbed dose calorimeter are described. Electrical calibration factors of thecalorimeter in the working temperature range from 10 to 35℃ are given. Thedistribution of dose rate to the distance in a 6oCo irradiation room is obtained.
关键词:Aluminitum;Absorbed dose;Calorimeter;γ ray;Computer data acquisition
摘要:High sensitive instrument neutron activation analysis is connected with highefficient nickel sulphide fire assay technique to establish the method for determingplatinum group elements(PGE) in geological materials. All PGE in some geologicalreference standard materials are analysed quantitatively. It is shown that this methodcan determine accurately all PGE at μg/kg concentration in geological materials.
关键词:platinum group element;Neutron activation analysis;Nickel sulphide fire assay
摘要:The structure of Fe73.5Cu1Nb3Si13.5B9 nanocrystalline material as a function ofannealing temperature was investigated by X-ray diffraction(XRD) and positronannihilation technique(PAT). The experimental results indicate that the amorphoussample startS nucleation and primary incrystallization at 480℃, and b.c.c. α-Fe(Si)solution separates out from the matrix. The amorphous diffusion peak decreases andthe crystalline diffraction peaks increase with annealing temperature. The crystallinefraction and the average distance among atoms in amorphous phase as a function ofannealing temperature are computed based on the diffraction spectra. The PATexperiments prove that the amorphous Phase at grain boundary mainly containing Nband B atoms exists in the sample after annealing at about 550℃。The change ofS-parameter is in accordance with that of the atomic average distance in amorphousphase with annealing temperature.
摘要:A rare meteorite, composed of a black part and a white part, was investigated bymeans of the 57Fe Mdssbauer effect. It is found .that both parts are composed ofolivine, pyroxene, troilite and kamacite, but with different contents. It is also provedthat this meteorite belongs to the equilibrated olivine-bronzite chondrite.
摘要:The yields of inorganic phosphate and base released from 5’-dTMP irradiated by30 keV N+ ion beam were investigated. The fluence effects of these yields and theinfluence with 0.1 mol/L NaOH treatment on them were presented. It was shown thatthe alkali treatment would not only increase the yield of inorganic phosphate, butalso damage and then split base released from the irradiated 5’-dTMP. When theirradiated samples were treated with 0.1 mol/L NaOH immediately, the yield ofinorganic phosphate was increased by a factor of 1.7 and the concentration of basedecreased to half of that in the sample’s water solution. Furthermore, the yield ofinorganic phosphate would increase by a factor of 2.8 after 40 min of alkalitreatment. Irradiation effects of ion beam were mainly direct ones and had a highervalue of G(Pi), greater than 0.44 molecule/100eV.
摘要:CaVSn:YIG was irradiated with 47 MeV/u carbon ions at Heavy Ion ResearchFacility of Lanzhou(HIRFL). The irradiation effects were studied by Mossbauerspectroscopy and positron lifetime measurement. The irradiation resulted in anisotropic distribution of the hyperfine magnetic field. No amorphous area Wasdetected in irradiated samples. The defects induced by irradiation were foundincreasing with the electron stopping power.
摘要:Briefly described its an iterative non-linear least-square fitting approach toanalyse overlapped peaks of energy-dispersive X-ray fluorescence spectra and alinear least-square fitting method for matrix correction of the spectrtum analysis. Acomputer software was compiled and successfully used to analyse multi-element rareearth samples.
摘要:ositron lifetime measurements are made in the as quenched state as well as inisochronal anneating cycle of the metaglasses Fe73.5Cu1Nb3Si13.5B9 andFe73.5Cu1Nb1.5Mo1.5Si13.5B9 respectively. The behaviors of lifetime are explained byinvoking the free volume model which affirms the existence of two kinds of freevolumes. The variation of positron lifetime as a function of annealing temperatureindicates the stages corresponding to structural relaxation and crystallization.