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1.中国科学院高能物理研究所 北京 100049
2.中国科学院大学 北京 100049
3.中国科学院光电研究院 北京 100094
[ "赵晓亮, 男, 1988年出生, 2013年毕业于山东大学, 现为博士研究生, 主要从事同步辐射光学技术研究", "ZHAO Xiaoliang, male, born in 1988, graduated from Shandong University in 2013, doctoral student, focusing on synchrotron radiation X-ray optics and techniques" ]
赵屹东, E-mail:zhaoyd@ihep.ac.cn ZHAO Yidong, E-mail: zhaoyd@ihep.ac.cn
收稿日期:2017-11-28,
修回日期:2018-01-11,
纸质出版日期:2018-04-10
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赵晓亮, 赵屹东, 唐坤, 等. 软X光低温辐射计[J]. 核技术, 2018,41(4):040101
Xiaoliang ZHAO, Yidong ZHAO, Kun TANG, et al. Soft X-ray cryogenic radiometer[J]. Nuclear techniques, 2018, 41(4): 040101
赵晓亮, 赵屹东, 唐坤, 等. 软X光低温辐射计[J]. 核技术, 2018,41(4):040101 DOI: 10.11889/j.0253-3219.2018.hjs.41.040101.
Xiaoliang ZHAO, Yidong ZHAO, Kun TANG, et al. Soft X-ray cryogenic radiometer[J]. Nuclear techniques, 2018, 41(4): 040101 DOI: 10.11889/j.0253-3219.2018.hjs.41.040101.
介绍了在北京同步辐射(Beijing Synchrotron Radiation Facility,BSRF)标定源的4B7B实验站上建立的一套软X光低温辐射计系统,用于测量从30nW~1μW范围的软X光功率。经多次实验发现:热沉和吸收体的温度稳定性以及热辐射背底涨落的控制是降低X光功率测量不确定度的关键。热沉的温度稳定是吸收体温度稳定的前提;吸收体上电加热功率根据待测X光功率调节,通过温度控制系统实现;低功率下X光功率测量不确定度受热辐射背底涨落的影响较大,通过优化热沉和吸收体的温度控制系统以及改进热链接的设计及工艺,使热沉的温度标准差控制在10 μK以下,吸收体的在15 μK以下。通过改善吸收体和热沉的受热环境,以及对通光管做特殊设计,控制热辐射背底的涨落在0.06 nW以内。对30 nW光功率的测试结果显示测量不确定度小于1%(
k
=1)。
Background
2
There is no commercial soft X-ray cryogenic radiometer available for 4B7B experiment station on Beijing synchrotron radiation facility (BSRF).
Purpose
2
This study aims to design and implement a soft X-ray cryogenic radiometer to measure the X-ray power from 30nW to 1 μW for BSRF.
Method
2
Intensive experiments were performed to find the key points to reduce the uncertainties of X-ray power measurement. The temperature stabilities of the heat sink
the absorber and the control of thermal radiation background fluctuation are principal factors influencing the accuracy whilst the temperature stability of the heat sink is the precondition of the absorber temperature stability. The heating power on the absorber is determined by the X-ray power and adjusted by the temperature control system. And for low X-ray power measurement
the uncertainties can be affected by the fluctuation of thermal radiation background.
Result & Conclusion
2
Through optimizing the temperature control system of the heat sink and the absorber
and improving the design technics of the heat link
the standard deviation of the heat sink can be kept under 10 μK
and the absorber is kept under 15 μK. The fluctuation of thermal radiation background can be stabilized less than 0.06 nW by improving the thermal environment and design special light pipes. The result of 30 nW X-ray power measurement shows that total uncertainties are less than 1% (
k
=1).
T Tanaka , M Kato , T Kurosawa , . First comparison of spectral responsivity in the soft X-ray region . Metrologia , 2012 . 49 ( 4 ): 501 - 506 . DOI: 10.1088/0026-1394/49/4/501 http://doi.org/10.1088/0026-1394/49/4/501 .
M Gerlach , M Krumrey , L Cibik , . Cryogenic radiometry in the hard X-ray range . Metrologia , 2008 . 45 ( 5 ): 577 - 585 . DOI: 10.1088/0026-1394/45/5/012 http://doi.org/10.1088/0026-1394/45/5/012 .
P Troussel , N Coron . BOLUX:a cryogenic electrical-substitution radiometer as high accuracy primary detector in the 150-11 000 eV range . Nuclear Instruments and Methods in Physics Research Section A:Accelerators, Spectrometers, Detectors and Associated Equipment , 2010 . 614 ( 2 ): 260 - 270 . DOI: 10.1016/j.nima.2009.12.043 http://doi.org/10.1016/j.nima.2009.12.043 .
E M Gullikson , R Korde , L R Canfield , . Stable silicon photodiodes for absolute intensity measurements in the VUV and soft X-ray regions . Journal of Electron Spectroscopy and Related Phenomena , 1996 . 80 313 - 316 . DOI: 10.1016/0368-2048(96)02983-0 http://doi.org/10.1016/0368-2048(96)02983-0 .
李华鹏. 基于同步辐射硬X射线探测器标定方法及关键技术研究[D]. 北京: 中国科学院高能物理研究所, 2017. http://ir.ihep.ac.cn/handle/311005/198878
LI Huapeng. Detector calibration method and key technology research based on synchrotron radiation hard X-rays[D]. Beijing: Institute of High Energy Physics, Chinese Academy of Sciences, 2017.
J E Martin , N P Fox , P J Key . A cryogenic radiometer for absolute radiometric measurements . Metrologia , 1985 . 21 ( 3 ): 147 - 155 . DOI: 10.1088/0026-1394/21/3/007 http://doi.org/10.1088/0026-1394/21/3/007 .
易 荣清 , 赵 屹东 , 王 秋平 , . 北京同步辐射装置4B7B软X射线标定束线的性能研究及应用 . 光学学报 , 2014 . 34 ( 10 ): 345 - 350 . DOI: 10.3788/AOS201434.1034002 http://doi.org/10.3788/AOS201434.1034002 .
Rongqing YI , Yidong ZHAO , Qiuping WANG , . Characteristic study and application of the soft X-ray beam line 4B7B on BSRF . Acta Optical Sinica , 2014 . 34 ( 10 ): 345 - 350 . DOI: 10.3788/AOS201434.1034002 http://doi.org/10.3788/AOS201434.1034002 .
T J Quinn , J E Martin . A radiometric determination of the Stefan-Boltzmann constant and thermodynamic temperatures between -40℃ and +100℃ . Philosophical Transactions of the Royal Society A:Mathematical, Physical and Engineering Sciences , 1985 . 316 ( 1536 ): 85 - 189 . DOI: 10.1098/rsta.1985.0058 http://doi.org/10.1098/rsta.1985.0058 .
A Gottwald , U Kroth , M Krumrey , . The PTB high-accuracy spectral responsivity scale in the VUV and X-ray range . Metrologia , 2006 . 43 ( 2 ): S125 - S129 . DOI: 10.1088/0026-1394/43/2/S25 http://doi.org/10.1088/0026-1394/43/2/S25 .
赵亚帅. 低温辐射计热沉的设计及其温度的控制[D]. 北京: 中国科学院高能物理研究所, 2017. http://ir.ihep.ac.cn/handle/311005/264631
ZHAO Yashuai. Design of heat sink and its temperature control in cryogenic radiometer[D]. Beijing: Institute of High Energy Physics, Chinese Academy of Sciences, 2017.
N P Fox , P R Haycocks , J E Martin , . A mechanically cooled portable cryogenic radiometer . Metrologia , 1995 . 32 ( 6 ): 581 - 584 . DOI: 10.1088/0026-1394/32/6/36 http://doi.org/10.1088/0026-1394/32/6/36 .
K D Stock , H Hofer , M White , . Lowest uncertainty direct comparison of a mechanically-cooled and a helium-cooled cryogenic radiometer . Metrologia , 2000 . 37 ( 5 ): 437 - 439 . DOI: 10.1088/0026-1394/37/5/20 http://doi.org/10.1088/0026-1394/37/5/20 .
H Rabus , V Persch , G Ulm . Synchrotron-radiation-operated cryogenic electrical-substitution radiometer as the high-accuracy primary detector standard in the ultraviolet, vacuum-ultraviolet, and soft X-ray spectral ranges . Applied Optics , 1997 . 36 ( 22 ): 5421 - 5440 . DOI: 10.1364/AO.36.005421 http://doi.org/10.1364/AO.36.005421 .
D A Pearson , Z M Zhang . Thermal-electrical modeling of absolute cryogenic radiometers . Cryogenics , 1999 . 39 ( 4 ): 299 - 309 . DOI: 10.1016/S0011-2275(99)00033-8 http://doi.org/10.1016/S0011-2275(99)00033-8 .
Scholze F, Brandt G, Mueller P, et al . High-accuracy detector calibration for EUV metrology at PTB[C]. Proceedings of the International Society for Optical Engineering, 2002, 4688 : 680-689. DOI: 10.1117/12.472342. http://dx.doi.org/10.1117/12.472342. http://proceedings.spiedigitallibrary.org/proceeding.aspx?articleid=880946
T R Gentile , J M Houston , J E Hardis , . National institute of standards and technology high-accuracy cryogenic radiometer . Applied Optics , 1996 . 35 ( 7 ): 1056 - 1068 . DOI: 10.1364/AO.35.001056 http://doi.org/10.1364/AO.35.001056 .
Carr S M, Woods S I, Jung T M, et al . PicoWatt infrared power measurement using an absolute cryogenic radiometer[C]. Proceedings of the International Society for Optical Engineering, 2009, 7298 : 72983Y-1. DOI: 10.1117/12.820290. http://dx.doi.org/10.1117/12.820290. http://www.researchgate.net/publication/253905462_Picowatt_infrared_power_measurement_using_an_absolute_cryogenic_radiometer
崔 明启 , 赵 屹东 , 郑 雷 , . 同步辐射软X射线光学实验平台的建立及其应用 . 中国激光 , 2010 . 37 ( 9 ): 2271 - 2277 . DOI: 10.3788/CJL20103709.2271 http://doi.org/10.3788/CJL20103709.2271 .
Mingqi CUI , Yidong ZHAO , Lei ZHENG , . Construction and applications of soft X-ray experimental platform on synchrotron radiation . Chinese Journal of Lasers , 2010 . 37 ( 9 ): 2271 - 2277 . DOI: 10.3788/CJL20103709.2271 http://doi.org/10.3788/CJL20103709.2271 .
M Gerlach , M Krumrey , L Cibik , . A cryogenic electrical substitution radiometer for hard X-rays . Nuclear Instruments and Methods in Physics Research Section A:Accelerators, Spectrometers, Detectors and Associated Equipment , 2007 . 580 ( 1 ): 218 - 221 . DOI: 10.1016/j.nima.2007.05.088 http://doi.org/10.1016/j.nima.2007.05.088 .
Z M Zhang , R U Datla , S R Lorentz , . Thermal modeling of absolute cryogenic radiometers . Journal of Heat Transfer , 1994 . 116 ( 4 ): 993 - 998 . DOI: 10.1115/1.2911476 http://doi.org/10.1115/1.2911476 .
S P Morozova , V A Konovodchenko , V I Sapritsky , . An absolute cryogenic radiometer for laser calibration and characterization of photodetectors . Metrologia , 1995 . 32 ( 6 ): 557 - 561 . DOI: 10.1088/0026-1394/32/6/31 http://doi.org/10.1088/0026-1394/32/6/31 .
J Lawrence , A B Patel , J G Brisson . The thermal conductivity of Kapton HN between 0.5 K and 5 K . Cryogenics , 2000 . 40 ( 3 ): 203 - 207 . DOI: 10.1016/S0011-2275(00)00028-X http://doi.org/10.1016/S0011-2275(00)00028-X .
阎 守胜 , 陆 果 . 低温物理实验的原理与方法 , : 北京 科学出版社 , 1985 .
Shousheng YAN , Guo LU . Principle and method of low temperature physics experiment , : Beijing Science Press , 1985 .
A Davies . Material properties data for heat transfer modeling in Nb 3 Sn magnets . Illinois Accelerator Institute , 2011 . 17 1 - 53 .
张 绪德 , 欧阳 峥嵘 . 低温温度计标定装置中测量引线传热分析 . 低温与超导 , 2008 . 36 ( 7 ): 9 - 11 . DOI: 10.3969/j.issn.1001-7100.2008.07.003 http://doi.org/10.3969/j.issn.1001-7100.2008.07.003 .
Xude ZHANG , Zhengrong OUYANG . The thermal analysis of gauge wire in cryogenic thermometer calibration facility . Cryogenics and Superconductivity , 2008 . 36 ( 7 ): 9 - 11 . DOI: 10.3969/j.issn.1001-7100.2008.07.003 http://doi.org/10.3969/j.issn.1001-7100.2008.07.003 .
Howell J R, Menguc M P, Siegel R. Thermal radiation heat transfer[M]. 5th ed. Chemical Rubber Company Press, Taylor & Francis Group, 2010.
D J Livigni , C L Cromer , T R Scott , . Thermal characterization of a cryogenic radiometer and comparison with a laser calorimeter . Metrologia , 1998 . 35 ( 6 ): 819 - 827 . DOI: 10.1088/0026-1394/35/6/5 http://doi.org/10.1088/0026-1394/35/6/5 .
Y K Cheng , J L Chern . Irradiance formations in hollow straight light pipes with square and circular shapes . Journal of the Optical Society of America A , 2006 . 23 ( 2 ): 427 - 434 . DOI: 10.1364/JOSAA.23.000427 http://doi.org/10.1364/JOSAA.23.000427 .
E Fu . Transmission of submillimeter waves through metal light pipes . Journal of the Optical Society of America B , 1996 . 13 ( 4 ): 702 - 705 . DOI: 10.1364/JOSAB.13.000702 http://doi.org/10.1364/JOSAB.13.000702 .
Xu N, Lin Y, Gan H, et al . Spectral responsivity calibration of silicon photodetectors using monochromator-based cryogenic radiometer[C]. Proceedings of International Symposium on Optoelectronic Technology and Application 2016, International Society for Optics and Photonics, 2016: 1015513. DOI: 10.1117/12.2245666 http://dx.doi.org/10.1117/12.2245666 .
Williams G P. X-ray data booklet[M]. Lawrence Berkeley National Laboratory, 2001.
S M Carr , S I Woods , T M Jung , . Experimental measurements and noise analysis of a cryogenic radiometer . Review of Scientific Instruments , 2014 . 85 ( 7 ): 075105 DOI: 10.1063/1.4883191 http://doi.org/10.1063/1.4883191 .
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