
浏览全部资源
扫码关注微信
1.中国科学技术大学 近代物理系 合肥微尺度物质科学国家实验室 合肥 230026
2.蚌埠学院理学院 蚌埠 233030
[ "陈昕, 男, 1991年出生, 2014年毕业于兰州大学, 现为硕士研究生, 研究方向为原子分子物理", "CHEN Xin, male, born in 1991, graduated from Lanzhou University in 2014, master student, focusing on atomic and molecular physics" ]
徐卫青, E-mail:xuwq412@mail.ustc.edu.cn ZHU Linfan, E-mail: xuwq412@mail.ustc.edu.cn
朱林繁, E-mail:lfzhu@ustc.edu.cn XU Weiqing, E-mail: lfzhu@ustc.edu.cn
收稿日期:2017-02-15,
修回日期:2017-03-09,
纸质出版日期:2017-05-10
移动端阅览
陈昕, 徐卫青, 徐龙泉, 等. 电子能量损失谱仪用中高能电子枪的研制[J]. 核技术, 2017,40(5):050102
Xin CHEN, Weiqing XU, Longquan XU, et al. Development of an electron gun operated at intermediate-high energies for electron energy-loss spectrometer[J]. Nuclear techniques, 2017, 40(5): 050102
陈昕, 徐卫青, 徐龙泉, 等. 电子能量损失谱仪用中高能电子枪的研制[J]. 核技术, 2017,40(5):050102 DOI: 10.11889/j.0253-3219.2017.hjs.40.050102.
Xin CHEN, Weiqing XU, Longquan XU, et al. Development of an electron gun operated at intermediate-high energies for electron energy-loss spectrometer[J]. Nuclear techniques, 2017, 40(5): 050102 DOI: 10.11889/j.0253-3219.2017.hjs.40.050102.
研制了一台电子能量损失谱仪用的中高能电子枪。其产生的电子与原子、分子发生碰撞,通过谱仪收集、分析散射电子的动量和能量,可以获得靶的电子结构和碰撞动力学信息。该电子枪结构简单,由热阴极、栅极、阳极、聚焦极和偏转板组成;电子能量可调范围大(1-3 keV),操作简单。为了获得最优的束流条件,利用SIMION电子光学软件模拟了电子发射源大小和初始发散角对靶点处的束斑大小和束流发散角的影响。在电子能量为1.5 keV条件下,实验检验给出在离电子枪出口27 mm处可获得束径约为0.95 mm、束流发散角约0.93°和束流强度6.27μA的电子束,满足电子能量损失谱仪的使用要求。
Background
2
In an electron energy-loss spectroscopy (EELS) experiment
the electron emitted by the electron gun collides with atoms and molecules
and the momentum and energy of the scattered electron are analyzed by EELS
then the information of electronic structure and collision dynamics of the target can be deduced.
Purpose
2
A well designed intermediate-high energy electron gun with small beam size and divergence angle is needed to satisfy the requirement of EELS.
Methods
2
To obtain the optimal beam condition
the electron optics software SIMION was utilized to simulate the space size and divergence angle of the electron beam at target position
the electron gun has a simple structure
i.e.
consisting of thermionic cathode
grid electrode
anode electrode
focus electrode and deflection plates. The tuning range of electron energy is wide (1-3 keV) and easy to operate.
Results
2
The beam size of 0.95 mm
divergence angel of 0.93°
and beam current of 6.27 μA of the constructed electron gun was obtained at 27 mm from the exit of electron gun at a beam energy of 1.5 keV.
Conclusion
2
An electron gun which satisfies the requirements of EELS has been developed.
M Inokuti . Inelastic collisions of fast charged particles with atoms and molecules-the Bethe theory revisited . Reviews of Modern Physics , 1971 . 43 ( 3 ): 297 - 347 . DOI: 10.1103/RevModPhys.43.297 http://doi.org/10.1103/RevModPhys.43.297 .
朱 林繁 , 凤 任飞 , 王 映雪 , . 高分辨快电子能量损失谱仪的改进 . 核技术 , 2001 . 24 ( 8 ): 663 - 667 . http://cpfd.cnki.com.cn/Article/CPFDTOTAL-HDZX199410001023.htm .
Linfan ZHU , Renfei FENG , Yingxue WANG , . New development of high resolution fast electron-energy-loss spectrometer . Nuclear Techniques , 2001 . 24 ( 8 ): 663 - 667 . http://cpfd.cnki.com.cn/Article/CPFDTOTAL-HDZX199410001023.htm .
H Ibach . Electron energy loss spectrometers , : Heidelberg Springer-Verlag , 1991 .
H Tanaka , M J Brunger , L Campbell , . Scaled plane-wave born cross sections for atoms and molecules . Reviews of Modern Physics , 2016 . 88 ( 2 ): 025004 DOI: 10.1103/RevModPhys.88.025004 http://doi.org/10.1103/RevModPhys.88.025004 .
D B Jones , R F C Neves , M C A Lopes , . Theoretical and experimental differential cross sections for electron impact excitation of the electronic bands of furfural . Journal of Chemical Physics , 2016 . 144 ( 12 ): 124309 DOI: 10.1063/1.4944615 http://doi.org/10.1063/1.4944615 .
T Y Suzuki , H Suzuki , S Ohtani , . Asymptotic behavior of apparent generalized oscillator strengths for optically forbidden transitions in rare-gas atoms . Physical Review A , 2007 . 75 ( 3 ): 032705 DOI: 10.1103/PhysRevA.75.032705 http://doi.org/10.1103/PhysRevA.75.032705 .
M Hoshino , Y Ishijima , H Kato , . Change in resonance parameters of a linear molecule as it bends:evidence in electron-impact vibrational transitions of hot COS and CO 2 molecules . The European Physical Journal D , 2016 . 70 ( 5 ): 1 - 13 . DOI: 10.1140/epjd/e2016-70085-9 http://doi.org/10.1140/epjd/e2016-70085-9 .
R Feng , G Cooper , G R Burton , . Absolute photoabsorption oscillator strengths by electron energy loss methods:the valence and S 2p and 2s inner shells of sulphur dioxide in the discrete and continuum regions (3.5-260 eV) . Chemical Physics , 1999 . 240 ( 3 ): 371 - 386 . DOI: 10.1016/S0301-0104(98)00364-4 http://doi.org/10.1016/S0301-0104(98)00364-4 .
Suzuki T Y.Studies for excitation in rare gas atoms by electron impact:asymptotic behaviors of generalized oscillator strengths[D].Tokyo:University of Electronic-Communications, 2000.
Silva F F Da , D Duflot , S V Hoffmann , . Electronic state spectroscopy of halothane As studied by ab initio calculations, vacuum ultraviolet synchrotron radiation, and electron scattering methods . Journal of Physical Chemistry A , 2015 . 119 ( 31 ): 8503 - 8511 . DOI: 10.1021/acs.jpca.5b05308 http://doi.org/10.1021/acs.jpca.5b05308 .
凤任飞. 高分辨快电子能量损失谱仪的研制[D]. 合肥: 中国科学技术大学, 1993.
FENG Renfei.Development of a high-resolution electron energy-loss spectrometer[D].Hefei:University of Science and Technology of China, 1993.
W Q Xu , J M Sun , Y Y Wang , . Generalized oscillator strengths and integral cross sections for the valence-shell excitations of oxygen studied by fast electron impact . Physical Review A , 2010 . 82 ( 4 ): 042716 DOI: 10.1103/PhysRevA.82.042716 http://doi.org/10.1103/PhysRevA.82.042716 .
M Vos , R P McEachran , L F Zhu . A comparison of the theoretical and experimental results for keV electron scattering from argon . Journal of Physics B:Atomic, Molecular and Optical Physics , 2014 . 47 ( 5 ): 055201 DOI: 10.1088/0953-4075/47/5/055201 http://doi.org/10.1088/0953-4075/47/5/055201 .
M Lin , Y W Liu , Z P Zhong , . Decay pathways of superexcited states of nitrous oxide . Chinese Physics B , 2014 . 23 ( 5 ): 053403 DOI: 10.1088/1674-1056/23/5/053403 http://doi.org/10.1088/1674-1056/23/5/053403 .
薛 冬冬 , 孙 秀宇 , 游 燕 , . 低能量电子枪的研发 . 真空电子技术 , 2016 . ( 1 ): 34 - 37 . http://www.cnki.com.cn/Article/CJFDTOTAL-ZKDJ201601012.htm .
Dongdong XUE , Xiuyu SUN , Yan YOU , . Development of a low energy electron gun . Vacuum Electronics , 2016 . ( 1 ): 34 - 37 . http://www.cnki.com.cn/Article/CJFDTOTAL-ZKDJ201601012.htm .
J M David , A D David . SIMION 8.0 user manual , : United States of America Scientific Instrument Services Inc , 2007 .
任 黎明 , 陈 宝钦 . 电子束曝光高斯分布束斑的Monte Carlo模拟 . 微细加工技术 , 2001 . 19 ( 3 ): 60 - 63 . http://www.cnki.com.cn/Article/CJFDTOTAL-WXJS200103012.htm .
Liming REN , Baoqin CHEN . Monte Carlo simulation of Gauss-distribution beam spot in electron beam lithography . Microfabrication Technology , 2001 . 19 ( 3 ): 60 - 63 . http://www.cnki.com.cn/Article/CJFDTOTAL-WXJS200103012.htm .
0
浏览量
25
下载量
0
CSCD
关联资源
相关文章
相关作者
相关机构
京公网安备11010802024621