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大连民族学院 物理与材料工程学院,大连,116600
[ "作者简介:安泰岩,男,1993年出生,2012年就读于大连民族学院攻读学士学位,研究领域为材料辐照损伤" ]
[ "通讯作者: 范红玉,E-mail: fanhy@dlnu.edu.cn E-mail:fanhy@dlnu.edu.cn" ]
纸质出版日期:2014-09-09
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安泰岩, 范红玉, 王 研, 等. 辐照温度对钨材料表面微结构的影响[J]. 核技术, 2014,37(9):090201
AN Taiyan, FAN Hongyu, WANG Yan, et al. Influence of irradiation temperature on the surface damage of tungsten[J]. Nuclear techniques, 2014, 37(9): 090201
安泰岩, 范红玉, 王 研, 等. 辐照温度对钨材料表面微结构的影响[J]. 核技术, 2014,37(9):090201 DOI: 10.11889/j.0253-3219.2014.hjs.37.090201.
AN Taiyan, FAN Hongyu, WANG Yan, et al. Influence of irradiation temperature on the surface damage of tungsten[J]. Nuclear techniques, 2014, 37(9): 090201 DOI: 10.11889/j.0253-3219.2014.hjs.37.090201.
本文采用100 eV的He+对钨进行辐照实验,考察了辐照温度变化(室温?800 °C)对钨材料的表面损伤作用。分别采用扫描电镜(Scanning Electron Microscope
SEM)、透射电镜(Transmission Electron Microscope
TEM)、导电原子力显微镜(Conductive Atomic Force Microscopy
CAFM)以及X射线衍射(X Ray Diffraction
XRD)技术对辐照后样品的微观形貌、内表面缺陷分布以及晶格结构进行了分析。结果表明,He+辐照后钨样品表面出现了纳米绒毛结构层,这种结构层组织间的间距及覆盖率都随辐照温度的增加而增加。纳米结构层会造成样品表面损伤,产生表面离域化,但不会引起钨晶相的改变。通过无损伤的CAFM检测技术证实了样品表面绒毛结构层的形成与样品内表面纳米尺寸He泡的形成有关。
Background: In fusion reactors
W suffers from the displacement damage caused by high energy neutrons
and surface damage
such as blistering
erosion
and sputtering caused by low-energy (tens of eV to several keV) and high-flux (1020?1024 m?2?s?1) helium and hydrogen ions. Purpose: The understanding of the behavior of W materials in fusion environment is a major issue of the material-related stake of fusion reactors. Methods: W samples were irradiated with low-energy (100 eV) and high-flux (6×1020 ions?m?2?s?1) He+ at a sample temperature changing from room temperature to 800 °C to a fluence of 1×1025 ions?m?2. Microscopic evolution of these samples was carried out using scanning electron microscopy (SEM)
transmission electron microscopy (TEM)
conductive atomic force microscopy (CAFM) and X-ray diffraction (XRD). Results: Analysis indicates that the nanometer-sized fibre-form structure is formed in the surface of W. The spacing and the covering degree of the nanostructure increase with the irradiation temperature. Nanostructure layer may cause the damage of W surface
resulting in surface delocalized
but does not cause a change in the crystal phase of tungsten. Conclusion: Non-destructive conductive atomic force microscopy gives the direct evidence that the forming of the nanometer-sized fibre-form structure is related to the nano-sized He bubbles. This is important for understanding the microstructure formation process of tungsten material. Abstract
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