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1. 中国科学院高能物理研究所同步辐射实验室
2. 首都师范大学应用化学系
3. 中国科学院高能物理研究所同步辐射实验室,北京,100039
4. ,北京,100037
纸质出版日期:2004-07-01
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[1]张静,谢亚宁,侯凯,胡天斗,刘涛.X射线吸收光谱技术中的滤光片研制[J].核技术,2004(07):497-500.
ZHANG Jing XIEYaning HOU Kai HUTiandou LIU Tao. Preparation and characteristics of X-ray filter in X-ray absorption spectroscopy techniques[J]. Nuclear techniques, 2004, (7): 497-500.
在同步辐射X射线吸收光谱(XAS)实验中
X射线滤光片用于吸收样品的康普顿散射和弹性散射
改善荧光信号的质量。我们将ZnO颗粒分散在聚氨酯溶液里
通过恰当的喷涂工艺
获得ZnO滤片。X射线衍射(XRD)
X射线荧光(XRF)及X射线吸收光谱(XAS)实验结果表明:在滤片制备过程中
ZnO结构保持不变。进一步地
ZnO滤片用于测量Ga2O3的Ga K边XAS谱
显示出好的信噪比。采用同样的方法还制备了其它X射线滤光片
表明这种X射线滤光片制备技术的可行性和实用性。
X-ray filters are used to absorb Compton and elastic scattering of samples
and to improve the quality of fluorescence signal in X-ray absorption spectroscopy (XAS) experiments. In the paper
ZnO filter is prepared by mixing ZnO powder into polyurethane
and then ZnO film is obtained by the spraying method. XRD (X-Ray Diffraction)
XRF(X-ray fluorescence) and X-ray absorption spectroscopy (XAS) experiments indicate that the ZnO structure remains in the preparation process of the filter. Further
the ZnO filter is used in the Ga K edge-XAS measurement of Ga2O3
showing a good signal noise ratio. Other X-ray filters can also be prepared by the same method
which proves to be practical.
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