
浏览全部资源
扫码关注微信
中国科学院高能物理研究所
收稿日期:1982-07-20,
纸质出版日期:1984-10
移动端阅览
冯锡璋, 罗世华, 赵珍兰, 等. 中子活化分析中钐与铀的相互干扰[J]. 核技术, 1984,07(5):59-60,26,76.
Xizhang Feng, Shihua Luo, Zhenlan Zhao, et al. Study of the interference between samarium and uranium in non-destructive neutron activation analysis[J]. Nuclear techniques, 1984, 07(5): 59-60,26,76.
在钐与铀的不破坏中子活化分析中主要测量46.4小时
153
Sm的103.2keV
γ
的光峰和56.4小时
239
Np的277.6keV
γ
的光峰。但是,在
239
Np的衰变中,由于内转换还有较大的几率发射99.5与103.7keV的X射线(
239
Pu),它们与
239
Np的106.1keV
γ
严重干扰钐的测量。用SCORPIO/SPECTRAN软件包中的
γ
谱单峰分析程序分析由SCORPIO-3000计算机程控Ge(Li)
γ
谱仪测得的经中子活化的纯铀的
γ
(X)谱,在所得的结果中,103.7keV光峰不出现,106.1keV光峰也显著偏小。若
153
Sm与
239
Np同时存在,则103keV光峰仍不出现
[1]
或虽出现但不准确,均严重影响钐的测量。用本实验室设计的重峰分析程序
[2]
,可以尚好地得出103与106keV峰。我们另外采用了一个剥谱法,它有助于解决以上的干扰问题,得出比较准确的钐的结果。
In presenta paper
the interference between Sm and U in non-destructive neutron activation analysis has been studied. When the radioactivities of
153
Sm and
239
Np are close to each other
the 103.2keV photopeak of
153
Sm and the 103.7keV photopeak of
239
Np (
239
Pu) do not appear correctly if the single-peak analysis is used. It seriously interfered the accurate measurement of Sm. The overlapping-peak-analysis program designed by our laboratory can be used to obtain the mixture of these two peaks. We use the stripping method. i. e. after stripping the spectrum of pure uranium
the mixed
γ
spectrum of Sm and U go through the single-peak or overlapping-peak analysis. By this way
we can get the pure 103.2keV photopeak of
153
Sm quite accurately. The stripping method can be used to strip the contributions of all the fission products of uranium. This also is the one of its advantages. The stripping method may have other applications in non-destructive neutron activation analysis.
冯锡璋 等 , 中子活化分析方法的研究 ( 未发表 )。
徐元彪 , 重峰分析程序 ( 未发表 )。
0
浏览量
26
下载量
0
CSCD
关联资源
相关文章
相关作者
相关机构
京公网安备11010802024621