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中国科学院上海原子核研究所
收稿日期:1987-05-25,
纸质出版日期:1989-10
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叶义芳, 要福增, 孙菊芳. 福美双-35S的制备[J]. 核技术, 1989,12(10):628-630.
Yifang Ye, Fuzeng Yao, Jufang Sun. Preparation of the 35S-labelled tetramethyl thiuram disulfide[J]. Nuclear techniques, 1989, 12(10): 628-630.
我们采用硫酸钠-
35
S作为放射性起始原料,其中经过硫化氢-
35
S和二硫化碳-
35
S二个中间产品,然后制得福美双-
35
S成品。化学和放化产率都达到85%以上(按二硫化碳计算),化学和放化纯度均为99%左右,比活度为0.16GBq/mmol。
The
35
S-labelled tetramethyl thiuram disulfide has been prepared by using sodium (
35
S) sulfate as primary material through forming the two intermediates (H
2
35
S and C
35
S
2
) . The chemical and radiochemical yield and purity are over 85% (based on CS
2
) and 99% respectively. The specific activity is 0.16GBq/mmol.
L. Elajarn , Acta Chem. Scand. , 3 ( 1949 ), 644 .
W. E. Mochel and J. H. peTerson , J. Amer. Chem. Soc. , 71 ( 1949 ), 1426 .
I. K. Khodzhaeva , Коллондный журнал , 23 ( 1961 ), 322 .
M. Bentov , Comm energie atomigue (Framce), Rappt, No. 832 , p. 3 ( 1958 ).
D. G. CLARKE et al ., Anal. Chem. , 23 ( 1951 ), 1842 .
佐藤敏郎 , Bull. Nat. Ins. Agr. Sei.(Japan), Series C(phytopathology and entomology) ,( 1960 ), 12 : 181
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