The parameters of Mössbauer spectral determination of two groups of samples are recorded. One group of samples is gold bearing fractural quartzvein type and altered type with different phases of mineralization

of which eleven are collected in different positions in midpart of No. 1 body of Xincheng goldmine and of which eight are collected in Shangdong Linglong mine and Xincheng mine. The other consists of 5 samples of intact rocks in the drill holes of ZK103 and ZK92 in profile 183. The corresponding variation can be observed in spectral line width and the probability of recoilless for pyrite samples with different phases of mineralization. The data are useful for studying of mechanism of mineralization of goldmine. On the other hand the paper is a primary exploration for giving a quantitative indication of mineralization and alteration.