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1.中国科学院上海原子核所
2.上海钢铁研究所
收稿日期:1980-06-03,
纸质出版日期:1982-04
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王振杰, 彭郁卿, 袁鹤令, 等. 用正电子湮灭技术测量塑性形变不锈钢中的位错密度[J]. 核技术, 1982,05(2):29-31.
Zhenjie Wang, Yuqing Peng, Heling Yuan, et al. The measurement of dislocation densities in plastically deformed stainless steel using positron annihilation[J]. Nuclear techniques, 1982, 05(2): 29-31.
自从1969年Bergersen和Stott
[1]
提出捕获模型以来,正电子湮灭技术广泛地应用于晶格缺陷的研究。1973年Baran和Rosen
[2]
第一次用多普勒展宽谱方法测量了冷加工镍、铜、银和金中的位错密度。Dlubek等人于1976年用角分布方法测量了镍中的位错密度及空位浓度随形变量的变化。他们的工作均限于纯金属。本工作用多普勒展宽谱方法测量了不同形变量下的海水用不锈钢中的位错密度,并给出了正电子比捕获速率。
The present work studied the dislocation densities in cold-rolled stainless steel by measuring the doppler broadening of the annihilation line. The specific trapping rate of dislocation for positron was given.
The γ-rays due to annihilation were detected by a pure germanium detector with the sensitive volume being 0.1cm
3
. The resolution of the system for 514keV γ-rays of
85
Sr was 1.2keV.
Dislocation densities were calculated according to the formulae for F. C. C. pure metal. Results showed that they increased from 9×10
8
cm
-2
to 5.7×10
11
cm
-2
as percent thickless reduced from 1% to 25%. The specific trapping rate for positrons was obtained: μ
d
=0.58cm
2
·s
-1
.
The results of present work made it clear that positron annihilation technique could be used to measure the densities of dislocation in alloys. However
the upper limit of dislocation density was about 10
-12
cm
-2
due to the saturation effect of the annihilation parameters.
B. Bergersen and M. I. Stott , Solid State Comm. , 7 , 1208 ( 1969 ).
J. Baran and M. Rosen , Phys. Stat. Sol., (A) 116 , 263 ( 1973 ).
G. Blubek et al . , Phys. Stat. Sol., (A) 34 , 737 ( 1976 ).
晏秀英 等 , 第一届全国核电子学和探测技术会议论文集 ( 1979 年).
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