摘要:BackgroundThe Shanghai synchrotron radiation facility (SSRF) is a third generation light source. It has been in operation for user experiment in decay mode since 2009. Meanwhile, the top-up operation is also under exploration in order to provide users with stable beam. A key technique for top-up mode is optimizing the injection efficiency by precisely controlling the injecting bunch charge. Therefore, it is essential to measure precisely the bunch charge at the high-energy transport line. The direct-current current transformers (DCCT) can measure the average beam current but can't measure the single bunch charge. Although the integrating current transformer (ICT) can measure the individual bunch charge, it is sensitive to different background noise with a resolution of less than 1% and even worse under low bunch charge case.PurposeThis study aims to improve the measuring resolution for the injected individual bunch charge by using cavity charge monitor.MethodsSince the cavity monitor has high sensitivity and high resolution, it will be used to extract the bunch charge information. Normally, the cavity monitor works at C-band frequency and the generated radio frequency signal (RF) has to be down-converted to intermediate frequency (IF) signal. Thus a dual-cavity monitor working at different frequencies was developed to realize the two RF signals self-mixing. Moreover, because of the limited signal sampling rate, the four channel signal splicing scheme with strict synchronous phase-locked sampling technique was addopted to further improve the sampling rate.ResultsThe experimental results show that IF signal amplitude is linear to the bunch charge quantity. Moreover, the test results presents the measuring sensitivity is better than 0.03%.ConclusionThe novel dual cavity bunch charge system works well and meets the requirement of injection bunch charge measurement.
摘要:BackgroundThe Soft X-ray Free-Electron Laser (SXFEL) is the fourth generation light source. The timing system is the key subsystem of the accelerator which can provide accurate timing trigger signal for the devices.PurposeThis study aims to design a timing system which can totally meet the requirements of SXFEL facility operation.MethodsAccording to the physical requirements and system physical equipments allocation of SXFEL, the hardware design of the timing system was based on the high precision pulse generator to realize high precision timing signals. The machine protection system (MPS) interface circuit and photoelectric converter for long distance transmission were developed as well. Experimental Physics and Industrial Control Systems (EPICS) was employed to perform the network-based distributed remote control system.Results & ConclusionsThe system works stably and reliably during the on line operation. The test results show that the jitter time is less than 150 ps, satisfying accelerator's requirements for timing system.
摘要:BackgroundX-ray photon correlation spectroscopy (XPCS) is a new technique for studying the small-scale relaxation dynamics of condensed matter by using the second order coherence of coherent X-ray scattering. It requires high coherence of incident light. The X-ray interference lithograph (XIL) beamline (BL08U) of Shanghai Synchrotron Radiation Facility (SSRF) uses elliptical polarization oscillator as light source, which has good coherence and high photon flux. It is suitable for the dynamics study of mesoscopic scale electrodes or magnetic micro-regions in ferroelectric and magnetic materials.PurposeThis study aims to design a set of photon correlation spectroscopy equipment based on soft X-ray.MethodsSoft X-ray from XIL of SSRF is used as coherent incident beam, and the secondary coherent light is collected, converted and amplified to perform autocorrelation operation. The effects of incident light energy and scattering angle on the scattering vector and period size of sample are discussed.ResultsWhen the spectral range is 90.5~93 eV and the hole diameter is 1 mm, the periodic scales of samples at different positions are 10~60 nm. The second-order correlation intensity function of detector arc region is deduced by using Gauss model, and it is used as a function of detection area, photon energy and time. The multiplicative noise of autocorrelation is suppressed by multilayer film polarization extinction.ConclusionThe development of this device provides a technical approach for better analysis of material dynamics information, and is of great significance.
摘要:BackgroundThe control and data acquisition system of the Shanghai synchrotron radiation facility (SSRF) hard X-ray microfocus beamline station was developed in the experiment physics and industrial control system (EPICS) environment. The existing fluorescence mapping system using EPICS software does not meet some specific requirements of fluorescence experiments.PurposeThis study aims to flexibly realize complicated fluorescent mapping techniques for SSRF hard X-ray microfocus beamline.MethodsBluesky and EPICS software were combined to design and implement a control and data acquisition system based on Python grammar structure. Functionalities such as motion control, light intensity detection and fluorescence signal acquisition were integrated in this system.ResultsThis system realizes real-time display of detected data and fluorescence mapping, adaptive step-size scanning, automatic calculation of peak statistics, continuous scanning of different samples in any spatial positions and two-dimensional square-spiral mapping.ConclusionThis proposed system allows users to perform complex fluorescence mapping with simple operation. It greatly improves the flexibility and efficiency of the experiment.
摘要:BackgroundThe main signal source is an essential part of digital low level radio frequency (LLRF) control system. It is used not only to generate the highly stable reference signals, but also to produce the high precision working clock required by the control system of LLRF.PurposeThis study aims to develope a high performance frequency synthesizer for Shanghai Synchrotron Radiation Facility (SSRF) so as to ensure high frequency system performance.MethodsTwo different techniques: phase-locked loop (PLL) and direct analog synthesis were employed to obtain the 500 MHz single frequency main signal source. Performance was measured and compared with the existing main signal source.ResultsThe experimental results show that the phase noise is -125 dBc/Hz@1 kHz and -132 dBc/Hz@1 kHz respectively, both of them meet the performance requirements of the RF system of SSRF.ConclusionDirect analog synthesis can be used to produce main signal source for SSRF and achieve better performance.
摘要:BackgroundNuclear graphite is easily impregnated by liquid molten salt under high pressure environment due to its porous structure, which will affect the mechanical properties of the nuclear graphite. In-situ real-time tensile synchrotron-based two dimensional X-ray diffraction (2D-XRD) plays an important role in exploring the interaction between graphite and molten salt.PurposeThis study aims to reveal the in-situ real-time interaction mechanism between IG-110 nuclear graphite and FLiNaK molten salt and the microscopic mechanism of material fracture under the external stress load.MethodsIn-situ real-time tensile synchrotron-based 2D-XRD at several fixed external forces, i.e., 0 N, 15 N, 21 N, 27 N and 32 N, were implemented to reveal the microstructure evolution of IG-110 nuclear graphite and FLiNaK salt during the tensile fracture process.ResultsDuring the tensile fracture process, the (002) diffraction peak of IG-110 nuclear graphite infiltrated with molten salt presents an obvious shift to a lower q, a gradually decreasing peak intensity and a gradually increasing full width at half maximum (FWHM). Meanwhile, the diffraction peaks of the FLiNaK salt also present a gradually decreasing peak intensity.ConclusionIn the process of tensile fracture, the larger the interlayer spacing, the worse the crystallinity of IG-110 nuclear graphite and FLiNaK salt are emerged.
关键词:Thorium molten salt reactor;IG-110 nuclear graphite;Molten salt impregnation;In-situ tensile synchrotron- based two dimensional X-ray diffraction
摘要:BackgroundWith the strong penetrability of fast neutrons, it is significant to use computed tomography(CT) neutron imaging to perform non-injury detection of large size samples. Fast neutron tomography is seldom performed because of the low efficiency of fast neutron detection and low signal to noise ratio of raw projected fast neutron image.PurposeThis study aims to fulfill non-injury detection of some big size samples by using fast neutron tomography technology.MethodsFirst of all, based on a pre-developed compact accelerator neutron source, a fast neutron tomography system was established. Then the raw projections of light and heavy material mixture sample from different angles were obtained. Fast neutron CT images were successfully reconstructed by algebraic reconstruction technique (ART) using the pre-processing projection.ResultsThe results show that the structure of the object consisting of copper and PTFE was clearly reconstructed and the flaws of different holes in light material were detected.ConclusionsThe fast neutron tomography can be realized by using small accelerator neutron source.
摘要:BackgroundIn normal operation or emergency, nuclear reactor can produce radioactive noble gases, the main components are 85Kr, 133Xe, 135Xe and 41Ar. It is of great significance to monitor the radioactivity of these mixed noble gases accurately for the operation of nuclear power plant.PurposeThis study aims to develop a 4π phoswich scintillator detector to measure the radioactivity of noble gases in online model.MethodsThe 4π phoswich scintillator detector consists of a sampling chamber, an inner plastic scintillator chamber for β measurement, and a CsI scintillator chamber for γ measurement. The pulse shaping discrimination (PSD) method is developed to distinguish the events between β, γ and β-γ coincidence events. Based on GEANT4 simulation toolkit, the performance of the detector, including the detection efficiency is investigated.ResultsThe simulation results show that both 0.3 mm plastic scintillator layer and a 20 mm CsI layer are necessary for measuring the radioactivity of noble gases. The size of sampling chamber should not be larger than ø50 mm×50 mm. Under these conditions, the detection efficiency for the above nuclides can be up to 90%.ConclusionsAccording to the simulation results, a composed 2-layer scintillation detector is designed, and its detection and recognition capability for different inert gases is studied. The comparison of these characteristics with actual calibration is the crucial step for this device.
摘要:BackgroundNeutron depth profiling (NDP) is a non-destructive near-surface analysis technique and it is widely used in characterization of polymers, semiconductors, alloys, lithium ion battery materials, photoelectric materials and many other materials.PurposeThis study aims is to develop NDP system to obtain the depth profiles of several crucial light nuclides (e.g., 6Li and 10B) in nearly any substrate.MethodsBased on the cold neutron beam of China advanced research reactor (CARR), a NDP system was developed with vacuum reached 3.4×10-5 Pa and neutron flux rate of 4.8×108 cm-2∙s-1. The standard reference material (SRM-2137) sample was used to test the performance of this NDP system. The measured α-particle spectrum was calculated by the inversion iterative algorithm to obtain the depth profiles of crucial elements.ResultsThe experimental results show that the simulation results of SRM-2137 agree well with the experimental results. The maximum error is less than 4% at each layer of 5 nm thickness. The peak depth is very close to the reference value (188 nm). The depth accuracy is 0.53%.ConclusionsEstablished CARR-NDP system and relevant experiments and data analysis techniques have been verified. The system will be further applied to investigating the lithium ion batteries, multilayer films and high-temperature alloys, etc.
摘要:BackgroundAfter the analog-to-digital converter (ADC) conversion, the baseline drift caused by CR differential circuit always exists. It increases the complexity of digital baseline estimation algorithm, and affects the real-time and accuracy of online baseline.PurposeThis study aims to improve the average method for extracting the digital baseline algorithm of random waveform signals in real-time.MethodsAn improved method of nuclear pulse digital baseline named average threshold method that can be implemented in field-programmable gate array (FPGA) was proposed. A measured signal with undershoot was taken as simulation nuclear pulse signal by disassembling and splicing to obtain a new signal with a fixed baseline value.ResultsThe baseline obtained by the average threshold method was consistent with the splicing baseline value. This algorithm exhibited strong real-time tracking effect while the baseline was changing.ConclusionThe average threshold method for real-time extraction of random waveform signals digital baseline algorithm can effectively calculate the baseline with less memory occupation and quick speed. The baseline value processed by the algorithm is stable, has a strong follow-up effect.
关键词:Nuclear signal with undershoot;Digital baseline;Average threshold method
摘要:BackgroundThe strong non-covalent interaction between streptavidin (STV) and biotin has been applied to various fields including molecular biology, immunology and biotechnology. The unique binding ability of STV to biotin is closely related to its structure. The crystal analysis results show that STV is a tetramer protein. Atomic force microscopy (AFM) plays an important role in studying the structure and function of proteins because it can provide morphological information of individual biomolecules in liquid environment. However, resolving STV with high-resolution AFM imaging remains challenge due to the small size and soft property.PurposeThis study aims to obtain high resolution single molecule STV images by AFM.MethodsWith modified biotin location on DNA origami, the addressable DNA origami was employed to selectively fix STVs. Then, AFM was used for image processing of STVs.ResultsThe single-molecule STV image at high-resolution was obtained. The observed STV showed an "hourglass-shaped" structure which consisted well with its crystal structure. At the same time, we noted that the STV morphology was susceptible to the effect of the loading force, indicating that it may be related to the flexibility of STVs.ConclusionThe simple and convenient method will provide a new way for studying the morphology and function of biomolecules.
关键词:Atomic force microscopy;Single-molecule;High-resolution imaging;Streptavidin;DNA origami
摘要:BackgroundThe failure compensation of superconducting cavity directly affects the stability of the proton beam, which is the focus of the study on accelerator-driven superconducting proton accelerator (C-ADS).PurposeThis study aims to design and implement an experimental platform to explore the results of the failure compensation of superconducting cavity.MethodsBased on experimental physics and industrial control system (EPICS) with embedded Linux system, programmable logic controller (PLC) was employed as the input/output controller (IOC) to communicate with the low level radio frequency (LLRF) of the cavity via the network of EPICS to obtain experimental results.ResultsSimulated failure data was quickly searched in IOC database, and the calculation of the time length of failure compensation at each stage was verified.ConclusionsThis experiment realized the rapid detection of failure of superconducting cavity and the automatic compensation operation of other cavities, which laid the foundation for practical application in future.
摘要:BackgroundWith advantages of large thermal capacity, good chemical stability, high temperature, molten salt has recently been widely used in concentrated solar thermal power plants, nuclear reactors, chemical engineerings, and other fields.PurposeThis study aims at the convective heat transfer characteristics and verifying the heat transfer laws of molten salt in a circular tube.MethodsFirst of all, a thermal experimental loop of Nitrate (KNO3-53%, NaNO2-40%,NaNO3-7%) was built as basic experimental facility. The turbulent convective heat transfer coefficient of molten salt in circular tube for fully developed was obtained by Wilson's correction method. Then the experimental results combining with the experimental data of five kinds of molten salt in the open literature were fitted to get the experimental correlation of molten salt in the range of 10 000<Re<50 000 and 4<Pr<26 for the turbulent flow in the round tube. Finally, comparisons of different kinds of molten salt with classical correlation Dittus-Boelter correlation, Sieder-Tate correlation, Hausen correlation and Gnielinski correlation were conducted.ResultsThe experimental data of molten salt agree well with the existing known relationship, and the deviation was below 25%.ConclusionThe results show that the heat transfer characteristics of the molten salts still conform to the classical heat transfer relationship.
摘要:BackgroundUNS N10003 alloy is considered to be the primary option of metal structural materials for the molten salt reactor (MSR). It will be affected by the extreme environments, i.e. high temperature, high neutron doses and corrosive coolant during the operation of MSR. Considering that the safe operation of MSR will mainly depends on the service performance of structural alloys, it is necessary to evaluate the performance of such kind of alloys in the complicated environments.PurposeThis study aims at understanding the effect of He bubbles on the corrosion properties of UNS N10003 alloy in molten salt environment.MethodsFirst of all, the 1.2 MeV high temperature He ion irradiation was performed on the UNS N10003 alloy at 650 oC. The irradiation fluence was set up to 5×1015 ions∙cm-2 and 5×1016 ions∙cm-2 respectively. Then, samples were immersed in a dry high-purity graphite crucible filled with 200 g FLiNaK salts and heated to 650 oC for 200 h. Finally, scanning electron microscopy (SEM) and transmission electron microscope (TEM) were employed to investigate the surface morphology, the distribution of elements and the microstructure, respectively. Nano-indentation technique was used to obtain the hardness.ResultsAt the dose of 5×1015 ions∙cm-2, there was not obvious difference in the surface morphology and distribution of element distribution of the corroded alloy with and without irradiation. While for the corroded alloy pre-irradiated with He ions at the dose of 5×1016 ions∙cm-2, large amount of holes were observed on the surface and the loss of Cr element was found from the bulk to the surface, which can be ascribed to the He bubbles formation. The hardness of irradiated alloy, corroded alloy, and corroded alloy pre-irradiated was 4.12 GPa, 2.65 GPa and 3.16 GPa, respectively.ConclusionHe bubbles formation play an important role on increasing the corrosion of UNS N10003 alloy. The hardness of irradiated and corroded alloy is lower than the irradiated alloy, and higher than of the corroded alloy. It is a combined effect of irradiation and corrosion.
关键词:Nickel based alloy;Ion irradiation;Molten salt corrosion;He bubbles
摘要:BackgroundCompared with the traditional pressurized-water reactor (PWRs) with low density coolant and loop layout, the lead-based reactor uses liquid heavy metal coolant and has the characteristics of pool layout.PurposeThis study aims at the impact and vibration modes of heavy metal coolant's sloshing to the reactor vessel and its internal components under a load of seismic.MethodsFirst of all, two-way fluid-structure coupling finite element method was applied to the seismic response analysis of liquid heavy metal reactor. Then the sloshing effect of coolant type, the support form, as well as the height-diameter ratio on the sloshing effect of coolant in the reactor container, were calculated and analyzed.ResultsThe calculation results show that the seismic response of liquid heavy metals is not equal to that of light coolant, and the fluid-dynamic viscosity is not significant for fluid-solid coupling of large-scale reactors. The different support forms have stress concentration at the support position and the overall performance is that the beam mode is not sensitive to the support form. The vibration modes stimulated by different liquid-filled ratios are similar, and the smaller the liquid-filled ratio, the more concentrated the maximum stress intensity point are on the bottom head.ConclusionThese results provide a parametric basis for the structural safety design of liquid heavy metal reactors.
关键词:Liquid heavy metal reactor;Coolant sloshing;Pool structure;Seismic response;Fluid-structure interaction