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福建省职业病与化学中毒预防控制中心 福州 350000
Received:20 February 2017,
Revised:08 April 2017,
Published:2017-09
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Yunhua QING, Pan LIU, Qishan ZHENG, et al. γ spectrometry analytical method of radionuclide[J]. Nuclear techniques, 2017, 40(9): 090502
Yunhua QING, Pan LIU, Qishan ZHENG, et al. γ spectrometry analytical method of radionuclide[J]. Nuclear techniques, 2017, 40(9): 090502 DOI: 10.11889/j.0253-3219.2017.hjs.40.090502.
在实验室仅存在混合刻度源条件下,探讨不同解谱方法对放射性核素活度估算的适用性。本文利用HPGe γ谱仪测量样品,并分别采用效率曲线法和相对比较法来分析样品中
241
Am、
60
Co、
137
Cs、
40
K核素活度。结果表明,若干扰核素对样品中待分析核素产生的影响可忽略,但对混合刻度源中相应的待分析核素影响较大时,经综合考虑,相对比较法所得结果优于效率曲线法;若干扰核素对样品中待分析核素产生的影响不可忽略,但对混合刻度源中相应的待分析核素影响不大时,与相对比较法相比,效率曲线法占优势。
Background:
Currently
mixture calibration sources
generally used in laboratory for saving cost
are limited in spectrum analysis.
Purpose:
The aim is to study the suitability of two spectrum analysis methods under the condition of mixture calibration source.
Methods:
In this work
four radionuclides
241
Am
60
Co
137
Cs
and
40
K
were measured by HPGe γ spectrometry and analyzed with relative comparison and efficiency curve methods under the condition of the mixture calibration source.
Results:
Relative comparison method can not calculate the radioactive activity of test nuclide influenced by interference nuclide
if interference nuclide could be ignored in mixture calibration source.
Conclusion:
Relative comparison method has an advantage comparing with efficiency curve method
if interference nuclide has no effect on test nuclide included in sample
but has a great effect on test nuclide included in mixture calibration source. However
efficiency curve method has an advantage comparing with relative comparison method. If interference nuclide has a great effect on test nuclide included in sample
but no effect appears on test nuclide included in mixture calibration source.
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