A Study on ￣（186）Re labelling of bleomycin

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A Study on ￣（186）Re labelling of bleomycin

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- A Study on ￣（186）Re labelling of bleomycin
- NUCLEAR TECHNIQUES Issue 4, (1995)
- 作者机构：
  
  中国工程物理研究院核物理与化学研究所
- 作者简介：
- 基金信息：
- DOI：
  CLC： R978.1
- Published：01 April 1995
- 稿件说明：
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[1]罗顺忠,蒲满飞,谯健,刘国平,刘中林,张昌英,付依备.~（186）Re标记博莱霉素的研究[J].核技术,1995(04):231-234.

A Study on ￣（186）Re labelling of bleomycin[J]. Nuclear techniques, 1995, (4).
[1]罗顺忠,蒲满飞,谯健,刘国平,刘中林,张昌英,付依备.~（186）Re标记博莱霉素的研究[J].核技术,1995(04):231-234. DOI：

A Study on ￣（186）Re labelling of bleomycin[J]. Nuclear techniques, 1995, (4). DOI：

摘要

采用Ｓｎ（Ⅱ）还原法，系统研究了反应条件对１８６Ｒｅ－ＢＬＭ形成的影响．结果表明：ｐＨ值对络合物产额影响最大．以葡萄糖酸钠为保护剂，可避免反应过程中铼的重新氧化，并建立了ｐＨ３—４．５时产额达９８％的制备条件．

Abstract

The influence of several factors on 186Re-BLM formation is investigated by means of Sn（II） reducing method. The results show that the labelling yield is mainly dependent on the pH value in reaction medium

and that sodium gluconate is a suitable protecting agent to avoid Re-oxidation of the reduced Re. The method for preparing 186-BLM is described with labelling yield up to 98% in the pH range from 3 to 4.5.

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