Synthesis of tritiated 12-（p -nitrobenzoyl） dihydroartemisinine

Yang Jianzhong Tang Guozhong

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Synthesis of tritiated 12-（p -nitrobenzoyl） dihydroartemisinine

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- Synthesis of tritiated 12-（p -nitrobenzoyl） dihydroartemisinine
- NUCLEAR TECHNIQUES Issue 8, (1992)
- 作者机构：
  
  1. 中国科学院上海原子核研究所
  2. 中国科学院上海原子核研究所,上海,201800
- 作者简介：
- 基金信息：
- DOI：
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- Published：01 August 1992
- 稿件说明：
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[1]杨建忠,唐国忠.氚标记对硝基苯甲酰还原青蒿素的合成[J].核技术,1992(08):510-512.

Yang Jianzhong Tang Guozhong. Synthesis of tritiated 12-（p -nitrobenzoyl） dihydroartemisinine[J]. Nuclear techniques, 1992, (8): 510-512.
[1]杨建忠,唐国忠.氚标记对硝基苯甲酰还原青蒿素的合成[J].核技术,1992(08):510-512. DOI：

Yang Jianzhong Tang Guozhong. Synthesis of tritiated 12-（p -nitrobenzoyl） dihydroartemisinine[J]. Nuclear techniques, 1992, (8): 510-512. DOI：

摘要

以青蒿素为起始原料

用钠硼氚还原制得氚标记还原青蒿素

然后与对硝基苯甲酰氯缩合反应

得到氚标记对硝基苯甲酰还原青蒿素粗产品

并经硅胶纸层析分离纯化

获得比活度为0.11TBq/mmol的纯品。

Abstract

Tritiated dihydroartemisinine was obtained by reduction of artemisinine with NaBT4

Then it was reacted with nitrobenzoylchloride. The tritiated product was purified by silica gel loaded paper chromatography. The specific activity was 0. 11TBq/mmol.

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