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1. 中国科学院上海应用物理研究所
2. 中国科学院研究生院
3. 台州学院物理系
Published:01 May 2009
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[1]谢巧玲,李勤涛,杨树敏,贺周同,周兴泰,朱德彰,巩金龙.金刚石薄膜为掩膜离子束室温溅射可控制备硅纳米圆锥阵列[J].核技术,2009,32(05):361-365.
XIE Qiaoling1, 2 LI Qintao1, 3 YANG Shumin1, et al. Controlled fabrication of Si nanocones by using diamond film as a mask under ion beam sputtering[J]. Nuclear techniques, 2009, 32(5): 361-365.
以金刚石薄膜为掩膜
采用低能Ar+束室温倾角溅射的方法制备密度和形貌可控的硅纳米圆锥阵列。扫描电子显微镜(SEM)结果表明
离子束溅射后得到的硅纳米圆锥密度与作为掩膜的金刚石薄膜颗粒密度相当;硅纳米圆锥的形貌与离子束入射角有密切关系
随着入射倾角由30°增大到75°
得到的硅纳米圆锥的锥角由73°减小到23°
其长径比从500nm/360nm增大到2400nm/600nm。由于金刚石比硅材料的溅射速率更低
因此以金刚石薄膜为掩膜可以制备较大长径比的硅纳米圆锥阵列;随着入射角的增大
离子束溅射诱导的表面原子有效扩散系数减小和溅射速率增大是硅纳米圆锥的锥角减小、长径比增大的主要原因。
Si nanocone array was fabricated under oblique ion beam bombardment on diamond film-masked Si substrates at room temperature.SEM images of the ion sputtered samples showed that the Si nanocone density was determined by density of the diamond particles on the Si substrate
and topography of the Si nanocones was closely linked with the beam incidence.By increasing the incidence angle from 30° to 75°
apex angle of the Si nanocone decreased from 73° to 23°
and aspect ratio of the Si nanocone increased from 500 nm/360 nm to 2400 nm/600 nm.It was believed that the formation of silicon nanocones using the diamond film mask was attributed to the lower sputtering rate of diamond compared to Si substrate.With increasing incidence angle
the decreasing apex angle and increasing aspect ratio of Si nanocone were attributed to decreased effective diffusion coefficiency and increased sputtering yield induced by the ion beams.
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