PIXE study on ancient glass samples of the Han Dynasty unearthed from Hepu county,Guangxi

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PIXE study on ancient glass samples of the Han Dynasty unearthed from Hepu county,Guangxi

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- PIXE study on ancient glass samples of the Han Dynasty unearthed from Hepu county,Guangxi
- NUCLEAR TECHNIQUES Issue 1, (2007)
- 作者机构：
  
  1. 中国科学院上海光学精密机械研究所
  2. 复旦大学,上海,201800
  3. 江西科技师范学院,上海,201800
  4. ,上海,200433
- 作者简介：
- 基金信息：
  
  国家自然科学基金资助项目(50272071);江西省科技厅(20041G0009600);教育厅2005年软科学项目(GJGZ[2005144])资助
- DOI：
  CLC： TL99
- Published：01 January 2007
- 稿件说明：
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[1]赵虹霞,李青会,干福熹,承焕生.广西合浦地区出土汉代古玻璃的质子激发X荧光分析[J].核技术,2007(01):27-33.

PIXE study on ancient glass samples of the Han Dynasty unearthed from Hepu county,Guangxi[J]. Nuclear techniques, 2007, (1): 27-33.
[1]赵虹霞,李青会,干福熹,承焕生.广西合浦地区出土汉代古玻璃的质子激发X荧光分析[J].核技术,2007(01):27-33. DOI：

PIXE study on ancient glass samples of the Han Dynasty unearthed from Hepu county,Guangxi[J]. Nuclear techniques, 2007, (1): 27-33. DOI：

摘要

采用改进的外束质子激发X射线荧光、电感耦合等离子体原子发射光谱分析等技术

对广西合浦地区出土的一批汉代古玻璃样品的化学成分和结构特性等进行了检测。结果表明:两汉时期

合浦地区的古代玻璃存在K2O-SiO2、PbO-BaO-SiO2、PbO-SiO2、Na2O-K2O-PbO-SiO2、（Na2O）K2O-CaO-SiO2等多种类型

但绝大多数为K2O-SiO2玻璃。表面风化可引起K2O-SiO2玻璃表面K2O等助熔剂的流失和富硅层的形成。综合化学成分以及器型特征

认为我国汉代K2O-SiO2玻璃制造技术可能受到同时期PbO-BaO-siO2玻璃制造技术和外来技术的双重影响。

Abstract

Combining the modified external-beam proton induced X-ray emission(PIXE)

inductively coupled plasma atomic emission spectrometry(ICP-AES)and other techniques

the chemical compositions

structures and other properties of some ancient glass samples of the Han Dynasty

which were unearthed from Hepu county

Guangxi

were determined.These glass samples can be classified to several glass systems

such as K2O-Si02

PbO-BaO-Si02

PbO-Si02

Na2O-K20-PbO-Si02 and (Na20)K20-CaO-Si02.But most of the samples belong to K20-Si02system glass.Due to the surface corrosion

the flux K20 in the surface of the K20-Si02glass Was lost

but with the relative enrichment of the Si02.Based on the characteristics of chemical composition and appearance of these samples

it is thought that

during the Han Dynasty

the making technique of the K20-Si02 glass in China Was influenced by the technique related to the PbO-BaO-Si02 glass from abroad.

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Related Author

申世放

承焕生

张斌

干福熹

李青会

LI Fei1 LI Qinghui1 GAN Fuxi1 ZHANG Bin2 CHENG Huansheng2 SHEN Shifang3 1

顾冬红

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Shanghai Institute of Optics and Fine Mechanics, the Chinese Academy of Sciences

Institute of Low Energy Nuclear Physics, Beijing Normal University

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