Study on new extractants for actinides and lanthanides separation (Ⅰ)  --syntheses and characterizations of 3H-pyrazol-3-thiones extractants

CAO Weiguo    1; 2    BAO Borong    1; 2    HUANG Wei  2  YANG Xingcun  1  HANG Jianzhong  2  CHEN Jie  2  1

doi:null

您当前的位置：

首页 >

文章列表页 >

Study on new extractants for actinides and lanthanides separation (Ⅰ) --syntheses and characterizations of 3H-pyrazol-3-thiones extractants

更新时间：2021-03-12

- Study on new extractants for actinides and lanthanides separation (Ⅰ) --syntheses and characterizations of 3H-pyrazol-3-thiones extractants
- NUCLEAR TECHNIQUES Issue 1, (2003)
- 作者机构：
  
  1. 中国科学院上海原子核研究所
  2. 上海大学化学系
  3. 上海大学化学系上海201800上海大学化学系上海,200436
  4. ,上海,201800
- 作者简介：
- 基金信息：
- DOI：
  CLC： O615
- Published：01 January 2003
- 稿件说明：
移动端阅览
[1]曹卫国,包伯荣,黄炜,杨兴存,杭建忠,陈杰.锕系、镧系元素分离中新萃取剂的研究(Ⅰ)——两种新型吡唑硫酮类萃取剂的合成及表征[J].核技术,2003(01):78-81.

CAO Weiguo 1, 2 BAO Borong 1, 2 HUANG Wei 2 YANG Xingcun 1 HANG Jianzhong 2 CHEN Jie 2 1. Study on new extractants for actinides and lanthanides separation (Ⅰ) --syntheses and characterizations of 3H-pyrazol-3-thiones extractants[J]. Nuclear techniques, 2003, (1): 78-81.
[1]曹卫国,包伯荣,黄炜,杨兴存,杭建忠,陈杰.锕系、镧系元素分离中新萃取剂的研究(Ⅰ)——两种新型吡唑硫酮类萃取剂的合成及表征[J].核技术,2003(01):78-81. DOI：

CAO Weiguo 1, 2 BAO Borong 1, 2 HUANG Wei 2 YANG Xingcun 1 HANG Jianzhong 2 CHEN Jie 2 1. Study on new extractants for actinides and lanthanides separation (Ⅰ) --syntheses and characterizations of 3H-pyrazol-3-thiones extractants[J]. Nuclear techniques, 2003, (1): 78-81. DOI：

摘要

本文通过酰基化、氯化、硫化反应合成两种新的酰代吡唑硫酮

即 1-苯基 - 3-甲基 - 4 - （2 -氯）苯甲酰基吡唑硫酮 - 5和 1-苯基 - 3-甲基 - 4 - （2 -氟）苯甲酰基吡唑硫酮 - 5。产物的结构用红外、氢核磁共振谱、质谱、元素分析及X衍射进行了表征。

Abstract

Two new extractants

4-dihydro-5-methyl-2-(2-chlorobenzoyl)-3H-pyrazol-3-thione (HCBMPPT) and 2

4-dihydro-5-methyl-2-(2-fluorobenzoyl)-3H-pyrazol-3-thione (HFBMPPT) were synthesized. The composition and structure of theses two compounds were confirmed by means of elemental analysis

mass spectrometry

1H NMR and X-ray crystal analysis.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Radio-synthesis and application research advance of amino acid molecular tracers labeling with 18F and 11C for tumor PET imaging

Synthesis and iodine-radiolabelling of peripheral benzodiazepine receptor tracer ¹³¹I-CLINDE

Synthesis of N,N’-didecanoylpiperazine and extraction behavior of U(Ⅵ)

Advances in preparation of 6 - [¹⁸F] fluoro- L - dopa

Related Author

唐刚华

李石磊

王朋

王淑侠

何山震

WANG Shuxia

TANG Ganghua

LI Shilei

Related Institution

广东省人民医院(广东省医学科学院)

中山大学附属第一医院

广东省人民医院广东省医学科学院

Department of Nuclear Medicine, Reiji Hospital, Medical School of Shanghai Jiaotong University, Shanghai 200127) 2

中国科学院上海生命科学院上海药物研究所

AI问答

Address：2019 Jialuo Road, Jiading, Shanghai, China Postal code：201800
Tel：021-39194977 Email：LHB@sinap.ac.cn
Technical support is provided by Beijing Founder electronics co., LTD 沪ICP备05005479号-1 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.
Total Visits：881003 Visits Today：530

⁰