PIXE analysis of Western Han dynasty ancient glasses unearthed in Yangzhou city

LI Qinghui GUDonghong GAN Fuxi ZHANG Bin MA Bo CHENG Huansheng

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PIXE analysis of Western Han dynasty ancient glasses unearthed in Yangzhou city

更新时间：2021-03-12

- PIXE analysis of Western Han dynasty ancient glasses unearthed in Yangzhou city
- NUCLEAR TECHNIQUES Issue 12, (2003)
- 作者机构：
  
  1. 中国科学院上海光学精密机械研究所
  2. 复旦大学应用离子束物理实验室,上海,201800
  3. ,上海,200433
- 作者简介：
- 基金信息：
- DOI：
  CLC： O657.3
- Published：01 December 2003
- 稿件说明：
移动端阅览
[1]李青会,顾冬红,干福熹,张斌,马波,承焕生.扬州西汉墓出土古玻璃的质子激发X荧光分析[J].核技术,2003(12):922-925.

LI Qinghui GUDonghong GAN Fuxi ZHANG Bin MA Bo CHENG Huansheng. PIXE analysis of Western Han dynasty ancient glasses unearthed in Yangzhou city[J]. Nuclear techniques, 2003, (12): 922-925.
[1]李青会,顾冬红,干福熹,张斌,马波,承焕生.扬州西汉墓出土古玻璃的质子激发X荧光分析[J].核技术,2003(12):922-925. DOI：

LI Qinghui GUDonghong GAN Fuxi ZHANG Bin MA Bo CHENG Huansheng. PIXE analysis of Western Han dynasty ancient glasses unearthed in Yangzhou city[J]. Nuclear techniques, 2003, (12): 922-925. DOI：

摘要

化学成分分析是中国古代玻璃研究中一个重要方面

可以为研究中国古代玻璃的起源和技术发展等提供科学的依据

有必要发展新的测试方法。质子激发X荧光（PIXE）技术是一种高灵敏度、非破坏性、多元素定量测定的分析方法。采用PIXE技术对扬州西汉墓出土的玻璃衣片进行了定量分析。结果表明:这些玻璃属中国自创的PbO-BaO-SiO

系玻璃;衣片由中心玻璃层和厚度不等的表面腐蚀层组成;腐蚀层比玻璃层含有相对较高的PbO、P

和CaO

而BaO和SiO

的含量则比玻璃层大大降低。对实验结果进行了讨论。

Abstract

Chemical composition analysis is one of the most important research aspects to provide scientific proof for the technical origin and development of Chinese ancient glass. Proton induced X-ray emission （PIXE） technique is a kind of multi-element quantitative analysis method with high sensitivity and without destruction of samples. Chemical composition of the Western Han dynasty glass garment flakes

which were excavated from Yangzhou city

was analyzed by PIXE

quantitatively. It was found that these glass flakes were attributed to PbO-BaO-SiO2 glass originated in China. These flakes all consist of a glass core and a corroded outer layer with different thickness. There are relatively higher PbO

P2O5 and CaO

while much lower BaO and SiO2 in the corroded layers than in the glass cores. The experimental results were discussed.

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Related Author

申世放

承焕生

张斌

LI Fei1 LI Qinghui1 GAN Fuxi1 ZHANG Bin2 CHENG Huansheng2 SHEN Shifang3 1

李青会

干福熹

李青会

承焕生

Related Institution

Shanghai Institute of Optics and Fine Mechanics, the Chinese Academy of Sciences, Shanghai 201800,China ) 2

重庆市博物馆

中国科学院上海光学精密机械研究所

复旦大学

江西科技师范学院

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