In order to investigate the change of defects in Fe
70
Cr
18
Mo
2
Si
1
B
9
microcrystal alloy
measurements of S-lineshape parameter of Doppler-broadened spectrum of positron annihilation were carried out for as-quenched ribbons treated at different temperatures
bulk samples prepared by crashing and hot-pressing
and bulk samples annealed at 1000℃
respectively. The results show that in the as-quenched ribbons there are three kinds of defects which are reduced in two steps during heat-treatment (at room temperature-600℃and 800—1000℃). In the bulk samples by crashing and hot-pressing a lot of stable defects are created with different amount when using different hot-pressing methods and the defects can hardly be removed even at high temperature up to 1000℃.
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references
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Nobuhiro Shiotani , Ptoc. 6th int. conf. on positron annihilation , U. S. A. , 1982 , p. 561 .