Preparation of the <sup>35</sup>S-labelled tetramethyl thiuram disulfide

Yifang Ye; Fuzeng Yao; Jufang Sun

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Preparation of the ³⁵S-labelled tetramethyl thiuram disulfide

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- Preparation of the ³⁵S-labelled tetramethyl thiuram disulfide
- Nuclear Techniques Vol. 12, Issue 10, (1989)
- 作者机构：
  
  中国科学院上海原子核研究所
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Received：25 May 1987，
  
  Published：1989-10
- 稿件说明：
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Yifang Ye, Fuzeng Yao, Jufang Sun. Preparation of the ³⁵S-labelled tetramethyl thiuram disulfide[J]. Nuclear techniques, 1989, 12(10): 628-630.
DOI：

Yifang Ye, Fuzeng Yao, Jufang Sun. Preparation of the ³⁵S-labelled tetramethyl thiuram disulfide[J]. Nuclear techniques, 1989, 12(10): 628-630. DOI：

摘要

我们采用硫酸钠-

S作为放射性起始原料，其中经过硫化氢-

S和二硫化碳-

S二个中间产品，然后制得福美双-

S成品。化学和放化产率都达到85%以上（按二硫化碳计算），化学和放化纯度均为99%左右，比活度为0.16GBq/mmol。

Abstract

The

S-labelled tetramethyl thiuram disulfide has been prepared by using sodium (

S) sulfate as primary material through forming the two intermediates (H

S and C

) . The chemical and radiochemical yield and purity are over 85% (based on CS

) and 99% respectively. The specific activity is 0.16GBq/mmol.

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references

L. Elajarn , Acta Chem. Scand. , 3 （ 1949 ）, 644 .

W. E. Mochel and J. H. peTerson , J. Amer. Chem. Soc. , 71 （ 1949 ）, 1426 .

I. K. Khodzhaeva , Коллондный журнал , 23 （ 1961 ）, 322 .

M. Bentov , Comm energie atomigue （Framce）, Rappt, No. 832 , p. 3 （ 1958 ）.

D. G. CLARKE et al ., Anal. Chem. , 23 （ 1951 ）, 1842 .

佐藤敏郎， Bull. Nat. Ins. Agr. Sei.（Japan）, Series C（phytopathology and entomology），（ 1960 ）, 12 ： 181

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Preparation of the 35S-labelled tetramethyl thiuram disulfide

DOI：

摘要

Abstract

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Keywords

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Preparation of the ³⁵S-labelled tetramethyl thiuram disulfide