The preparation of [5,6 (n) -3H] prostaglandin E1 and [5,6(n)-3H] prostaglandin A1

Rongzhen Cao; Nianbao Zhang; Yuanlong Yie

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The preparation of [5,6 (n) -³H] prostaglandin E₁ and [5,6(n)-³H] prostaglandin A₁

更新时间：2022-08-16

- The preparation of [5,6 (n) -³H] prostaglandin E₁ and [5,6(n)-³H] prostaglandin A₁
- Nuclear Techniques Vol. 05, Issue 2, (1982)
- 作者机构：
  
  中国科学院上海原子核研究所
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Received：07 March 1981，
  
  Published：1982-04
- 稿件说明：
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Rongzhen Cao, Nianbao Zhang, Yuanlong Yie. The preparation of [5,6 (n) -³H] prostaglandin E₁ and [5,6(n)-³H] prostaglandin A₁[J]. Nuclear techniques, 1982, 05(2): 58-61.
DOI：

Rongzhen Cao, Nianbao Zhang, Yuanlong Yie. The preparation of [5,6 (n) -³H] prostaglandin E₁ and [5,6(n)-³H] prostaglandin A₁[J]. Nuclear techniques, 1982, 05(2): 58-61. DOI：

摘要

氚标记前列腺素国外已广泛用于前列腺素的放射免疫测定及基础代谢研究，对于它的重要意义本文不再重述

［1］

。

Abstract

6(n)-

H] prostaglandin E

was prepared by the catalytic reduction of prostaglandin E

. RhCl(pph

)

was used as a catalyst.

The specific activity of the product was 41Ci/m

. Its radiochemical purity was over 95%. The labelled compound can be used in the radioimmunoassay. [5

6(n)-

H]prostaglandin A

was prepared by the acidification of [5

6(n)-

H] prostaglandin E

关键词

Keywords

references

曹蓉珍和张年宝，核技术， 1 , 67 （ 1979 ）.

G. K. Koch and J. W. Dalenberg J. Label. Compounds , 6 , 395 ( 1970 ).

中国科学院上海有机化学研究所一室等，化学通报， 1 , 36 （ 1976 ）.

J. A. Osborn et al . , J. Chem. Soc ., A , 1711 （ 1966 ）.

E. Änggard and B. Samuelsson , J. Biol. Chem. , 239 , 4097 ( 1964 ).

S. Bergstron , J. Biol. Chem. , 238 , 3555 ( 1963 ).

N. H. Andersen , J. Lipid Res. , 10 , 320 ( 1969 ).

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